HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-methyl-N-[(2-methyl-6-pyridinyl)methyl]-2-propenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 2-(6-Methylpyridin-2-yl)ethan-1-amine | HCID 1514165 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-methyl-N-[(2-methyl-6-pyridinyl)methyl]-2-propenamide | HCID 19826106 | — |
Reaction Steps
The title compound was prepared according to the method of Example 6 from 6-methyl-2-picolylmethylamine (4.27 g, 0.035 mole), acryloyl chloride (3.15 g, 0.035 mole) and triethylamine (21 ml) in methylene chloride. Analysis calc. for C11H14N2O(190.24): Calc.: C, 69.44; H, 7.42; N, 14.72. Found: C, 69.41; H, 7.53; N, 14.68.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030642 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-3261731c980047bf80a0c6dfc02c0a2c |
| Source note | uspto-grants-1991_07 |