HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 13822941, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Methyl[2-(pyridin-4-yl)ethyl]amine | HCID 143276 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13822941 | HCID 13822941 | — |
Reaction Steps
The title compound was prepared according to the method of Example 3 from 4-[β-(methylamino)ethyl]pyridine (4.76 g, 0.035 mole), acryloyl chloride (3.15 g, 0.035 mole) and triethylamine (21 ml) to yield 3.4 g of product, m.p. ca. 129°-132° C. Analysis calc. for C11H14N2O(190.24): Calc.: C, 69.45; H, 7.42; N, 14.72. Found: C, 69.79; H, 7.62; N, 14.20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030642 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-086226f0b36941319209120b794a7985 |
| Source note | uspto-grants-1991_07 |