2,6-Dichloro-4-mercaptophenol → HCID 13822939, compound

Participants

Reaction Steps

The title compound was prepared according to the method of Example 4, from N-methyl-N-[2-(2-pyridinyl)-ethyl]-2-propenamide (2.5 g. 0.013 mole), 2,6 dichloro-4-mercaptophenol (2.56 g, 0.013 mole) and triethylamine (5 ml), m.p. about 120°-123° C. Analysis calc. for C17H18N2O2Cl2S (385.31): Calc.: C, 52.97; H, 4.71; N, 7.27; Cl, 18.40; S, 8.32. Found: C, 53.18; H, 4.89; N, 7 34; Cl, 18.59; S, 8 05.

Provenance & Evidence