2,6-Dichloro-4-mercaptophenol → HCID 13822939, compound

HRID 1086464Notes

Reaction equation

HRID 1086464 reaction equation
[CH3:1][N:2]([CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][N:10]=1)[C:3](=[O:6])[CH:4]=[CH2:5].[Cl:15][C:16]1[CH:21]=[C:20]([SH:22])[CH:19]=[C:18]([Cl:23])[C:17]=1[OH:24]>C(N(CC)CC)C>[Cl:15][C:16]1[CH:21]=[C:20]([S:22][CH2:5][CH2:4][C:3]([N:2]([CH3:1])[CH2:7][CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][N:10]=2)=[O:6])[CH:19]=[C:18]([Cl:23])[C:17]=1[OH:24]

Participants

4

Reactant 2

HCID 30163632,6-Dichloro-4-mercaptophenolHCID 13822937HCID 13822937, compound

Product 1

HCID 13822939HCID 13822939, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound was prepared according to the method of Example 4, from N-methyl-N-[2-(2-pyridinyl)-ethyl]-2-propenamide (2.5 g. 0.013 mole), 2,6 dichloro-4-mercaptophenol (2.56 g, 0.013 mole) and triethylamine (5 ml), m.p. about 120°-123° C. Analysis calc. for C17H18N2O2Cl2S (385.31): Calc.: C, 52.97; H, 4.71; N, 7.27; Cl, 18.40; S, 8.32. Found: C, 53.18; H, 4.89; N, 7 34; Cl, 18.59; S, 8 05.

Sources & evidence

ORD record
ord-3a2fd01301464f2c9c8c0a6d78a9b98a
Source dataset
uspto-grants-1991_07
Patent number
US05030642

Reaction notes

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