HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13822937, compound → 3-[(2'-hydroxy[1,1':3',1"-terphenyl]-5'-yl)-thio]-N-methyl-N-[2-(2-pyridin-yl)ethyl]propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13822937 | HCID 13822937 | — |
| Reactant | 5'-Mercapto[1,1':3',1"-terphenyl]-2'-ol | HCID 14989168 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-[(2'-hydroxy[1,1':3',1"-terphenyl]-5'-yl)-thio]-N-methyl-N-[2-(2-pyridin-yl)ethyl]propanamide | HCID 19826109 | — |
Reaction Steps
The title compound was prepared according to the method of Example 4 from the thiol of Example 16(2.78 g, 0.01 mole), N-methyl-N-[2-(2-pyridinyl)ethyl]-2-propenamide (1.90 g, 0.01 mold) and triethylamine (1.2 ml). Analysis calc. for C29H28O2N2S (468.54): Calc.: C, 74.32; H, 6.02; N, 5.98. Found: C, 73.93; H, 6.04; N, 6.16.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030642 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-161c26c98a5143b090297f1486396030 |
| Source note | uspto-grants-1991_07 |