HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-chlorobenzamide → 2-methyl-6-chloro-5H-thiazolo-(2,3-b)-quinazolin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-chlorobenzamide | HCID 13675968 | — |
| Reactant | 2-Bromo-5-methyl-1,3-thiazole | HCID 21906106 | — |
| Product | 2-methyl-6-chloro-5H-thiazolo-(2,3-b)-quinazolin-5-one | HCID 19826342 | 78.1% |
Reaction Steps
10.2 g of 6-chloroanthranilamide and 10.74 g of 2-bromo-5-methylthiazole were stirred at 140° C. for 2 hours. After working up in the conventional manner there was obtained 11.7 g (78%) of the above compound; m.p. 235°-236° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030727 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-cc7be1eb2d764f198dbfe2b4c532da35 |
| Source note | uspto-grants-1991_07 |