HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14483347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 18646051 | HCID 18646051 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14483347 | HCID 14483347 | 101% |
Reaction Steps
To 20 ml solution of 2.18 g (5 mmols) N-carbobenzoxy-β-bromoalanine p-nitrobenzyl ester in tetrahydrofuran, 1.01 g (10 mmols) triethylamine was added and the mixture was stirred at room temperature for 30 minutes. Solvent was removed under reduced pressure, water was added and the crystals which formed were filtered to obtain 1.80 g (yield 100%) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030732 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-d8b33bb7781b49f9a59cedbd35c2f551 |
| Source note | uspto-grants-1991_07 |