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HRID1086657

反应详情

EQUATION

反应方程式

HRID 1086657 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(N=C=O)c1cccc(C(C)(C)N=C=O)c1
HCID17719

1,3-Bis(2-isocyanato-2-propyl)benzene

C14H16N2O2

结构：NCCOCCOCCOCCO
HCID160103

Ethanol, 2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy]-

C8H19NO4

PRODUCTS

生成物

1
结构：CC(C)(N=C=O)c1cccc(C(C)(C)N=C=O)c1.NCCOCCOCCOCCO
HCID131716948

未命名化合物

PROCEDURE

实验过程

To a one-liter 3-necked flask equipped with a thermometer, stirrer, dropping funnel and a nitrogen inlet was 122 g (0.5M) of TMXDI (from American Cyanamid). Then 193 g (1.0 mole) of tetraethylene glycol monoamine was added over a 50 minute period keeping the temperature below 36° C. A clear viscous product was obtained.

WORKUP

后处理

  1. customTo a one-liter 3-necked flask equipped with a thermometer, stirrer
  2. customthe temperature below 36° C
  3. customA clear viscous product was obtained