HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Bis(1-isocyanato-1-methylethyl)benzene → Tmxdi T4egma
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Bis(1-isocyanato-1-methylethyl)benzene | HCID 17719 | — |
| Reactant | Ethanol, 2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy]- | HCID 160103 | — |
| Product | Tmxdi T4egma | HCID 131716948 | — |
Reaction Steps
To a one-liter 3-necked flask equipped with a thermometer, stirrer, dropping funnel and a nitrogen inlet was 122 g (0.5M) of TMXDI (from American Cyanamid). Then 193 g (1.0 mole) of tetraethylene glycol monoamine was added over a 50 minute period keeping the temperature below 36° C. A clear viscous product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05030754 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-cc123ef2ccd84e13a0072d2a80df34b2 |
| Source note | uspto-grants-1991_07 |