HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 178444466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | HCID 178444473 | HCID 178444473 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178444466 | HCID 178444466 | 60.3% |
Reaction Steps
2.9 g of 4-hydroxybenzaldehyde, 5.0 g of (E)-3-(trans-4-pentylcyclohexyl)allyl alcohol, 4.1 g of diethyl azodicarboxylate, 6.2 g of triphenylphosphine and 100 ml of tetrahydrofuran were reacted in an analogous manner to Example 1 to give 4.5 g of 4-[(E)-3-(trans-4-pentylcyclohexyl)allyloxy]benzaldehyde (m.p. 54-55° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05032312 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-b631cb2abb95495f9ed9cf683b153ab4 |
| Source note | uspto-grants-1991_07 |