HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Nitro-1-tetralone → 7-Amino-1,2,3,4-tetrahydronaphthalen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Nitro-1-tetralone | HCID 38445 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 7-Amino-1,2,3,4-tetrahydronaphthalen-1-one | HCID 327177 | — |
Reaction Steps
A solution of 2 g (0.0105 mole) 7-nitro-1-tetralone in 120 ml ethanol was hydrogenated under <5 psi H2 pressure using Raney Ni as catalyst. The solution was filtered with the aid of super gel and concentrated under reduced pressure to give the 7-amino-1-tetralone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05032598 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-61fe34ea4363434b8cdd645cf320cbb4 |
| Source note | uspto-grants-1991_07 |