HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 15752838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 15752834 | HCID 15752834 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15752838 | HCID 15752838 | 79.3% |
Reaction Steps
A solution of 0.20 g (0.62 mmol) of the resultant compound of Example 187 in methanol was treated with sodium methoxide and stirred at ambient temperature for 2 h. The solvent was removed in vacuo, and the residue was acidified with IN HCl, extracted with chloroform, and concentrated to give 159 mg of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05032577 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-e502e3ebf2754cdb97b228c8e5aeba8e |
| Source note | uspto-grants-1991_07 |