関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dibutyltin oxide | HCID 61221 | — |
| 反応物 | Isooctylthioglycolate | HCID 21895674 | — |
| 生成物 | Acetic acid,2,2'-[(dibutylstannylene)bis(thio)]bis-, 1,1'-diisooctyl ester | HCID 21981422 | 102.6% |
反応手順
A suitable reactor was charged with 248.7 grams (1.0 mole) of dibutyltin oxide and 425.4 grams (2.05 moles) of isooctylthioglycolate of commercial purity. The reaction mixture was heated under vacuum, with agitation, to about 110° C. while distilling off water of reaction. On cooling and filtering, 656.1 grams of dibutyltin bis(isooctylthioglycolate) was obtained as an oily liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05032634 |
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| 出典データセット | uspto-grants-1991_07 |
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| ORD ID | ord-61bb24366e584ffa8ba8a957788f3b68 |
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| 出典メモ | uspto-grants-1991_07 |
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