HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 4-[2-[Ethyl[3-(propylsulfinyl)propyl]amino]-1-hydroxyethyl]-benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-[2-[Ethyl[3-(propylthio)propyl]amino]-1-hydroxyethyl]-benzonitrile | HCID 15158816 | — |
| Product | 4-[2-[Ethyl[3-(propylsulfinyl)propyl]amino]-1-hydroxyethyl]-benzonitrile | HCID 15158817 | 73.9% |
Reaction Steps
0.9 g of 4-[2-[ethyl[3-(propylthio)propyl]amino]-1-hydroxyethyl]-benzonitrile was oxidized with 0.7 g of m-chloroperbenzoic acid in analogy with example 2. Yield: 0.7 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05034411 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-1ba397ba134e4517b1268dba87bc6762 |
| Source note | uspto-grants-1991_07 |