Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 10066899 | HCID 10066899 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19817740 | HCID 19817740 | 85.3% |
Reaction Steps
A mixture of 5'-acetyl-2'-(2,4-difluorophenylthio)methanesulfonanilide (1 g) and nitric acid (248 mg) in acetic acid (5 ml) was stirred at 80° C. for 1 hour. The reaction mixture was evaporated to dryness. The residue was washed with ethanol to give yellow crystals of 5'-acetyl-2'-(2,4-difluorophenylthio)-4'-nitromethanesulfonanilide (0.96 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05034417 |
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| Source dataset | uspto-grants-1991_07 |
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| ORD ID | ord-ad67e8af750c4b49a2d204677b4e2cae |
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| Source note | uspto-grants-1991_07 |
|---|
