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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1087375Generated: October 31, 2026

Acetic Anhydride → HCID 19816902, compound

https://huagongshe.com/reaction/1087375

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 19816950HCID 19816950—
SolventPyridineHCID 1049—
ProductHCID 19816902HCID 19816902—

Reaction Steps

A mixture of 1 g of 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-amino-2H-1,3-benzoxazine, 10 ml of acetic anhydride and 10 ml of pyridine is left to stand at 20° for 16 hours. The mixture is evaporated, and the residue is purified by chromatography to give 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-acetamido-2H-1,3-benzoxazine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05036068
Source datasetuspto-grants-1991_07
ORD IDord-4ea0eccd5e004898912a8d51dced724d
Source noteuspto-grants-1991_07