HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 19816902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19816950 | HCID 19816950 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19816902 | HCID 19816902 | — |
Reaction Steps
A mixture of 1 g of 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-amino-2H-1,3-benzoxazine, 10 ml of acetic anhydride and 10 ml of pyridine is left to stand at 20° for 16 hours. The mixture is evaporated, and the residue is purified by chromatography to give 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-acetamido-2H-1,3-benzoxazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036068 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-4ea0eccd5e004898912a8d51dced724d |
| Source note | uspto-grants-1991_07 |