HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 19816871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178430675 | HCID 178430675 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19816871 | HCID 19816871 | — |
Reaction Steps
A mixture of 296 mg of 2,2-dimethyl-4-(6-hydroxy-3-pyridazinyloxy)-6-cyano-2H-1,3-benzoxazine, 1 g of K2CO3,0.65 ml of dimethyl sulfate and 16 ml of DMF is boiled for 3 hours and subjected to customary work-up. 2,2-Dimethyl-4-(6-methoxy-3-pyridazinyloxy)-6-cyano-2H-1,3-benzoxazine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036068 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-b0758b595fb545ba849d041fb95e4d23 |
| Source note | uspto-grants-1991_07 |