HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 15661028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 13151869 | HCID 13151869 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15661028 | HCID 15661028 | — |
Reaction Steps
To a solution of 2-acetyl-10,11-dihydro-dibenzo[b,f]thiepin-7-carboxylic acid (U.S. Pat. No. 4,536,507 (1985)) (600 mg, 2.01 mmol) in ethyl acetate (10 mL), was added dropwise a solution of diazomethane in ether until the yellow coloration persisted. Evaporation of the solvent gave the crude title compound as a solid which was used as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036067 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-33b3b866504b46938a7cba5eb4609c1e |
| Source note | uspto-grants-1991_07 |