Epichlorohydrin → 2212-07-9

HRID 1087404Notes

Reaction equation

HRID 1087404 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[OH:9].C(=O)([O-])[O-].[K+].[K+].Cl[CH2:17][CH:18]1[O:20][CH2:19]1>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[O:9][CH2:17][CH:18]1[O:20][CH2:19]1

Participants

4

Reactant 3

HCID 7835EpichlorohydrinHCID 84492,4-DichlorophenolHCID 11430Potassium Carbonate

Product 1

HCID 2193952212-07-9

Procedure

A mixture containing 81.5 g of 2,4-dichlorophenol in 120 g of 1-chloro-2,3-epoxypropane and 138 g of potassium carbonate is refluxed for 10 hours.

Workup

  1. temperatureis refluxed for 10 hours

Sources & evidence

ORD record
ord-d82f55d58b854b2e8e9f656bfbfa648c
Source dataset
uspto-grants-1991_07
Patent number
US05036077

Reaction notes

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