2'-Hydroxybenzophenone → HCID 15718520, compound

HRID 1087713Notes

Reaction equation

HRID 1087713 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[O:9].[CH3:16][N:17]([CH3:21])[C:18](Cl)=[S:19]>>[CH3:16][N:17]([CH3:21])[C:18](=[S:19])[O:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:9])[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 83482'-HydroxybenzophenoneHCID 27871Dimethylthiocarbamoyl chloride

Product 1

HCID 15718520HCID 15718520, compoundYield 82%

Procedure

Following the procedure described in Preparation Ia and starting from 9.5 g (0.048 mol) of 2-hydroxyphenyl phenyl methanone and 10.3 g (0.083 mol) of dimethylthiocarbamoyl chloride, 11.2 g of the expected product are obtained (yield: 82%).

Workup

  1. customdescribed in Preparation Ia

Sources & evidence

ORD record
ord-d7528a5cdc7b4c729d8ce45012770202
Source dataset
uspto-grants-1990_10
Patent number
US04960758

Reaction notes

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