HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoanisole → 2-Bromo-2'-methoxybenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoanisole | HCID 11358 | — |
| Reactant | 2-Bromobenzoyl chloride | HCID 23542 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Product | 2-Bromo-2'-methoxybenzophenone | HCID 15718541 | 66% |
Reaction Steps
Following the Procedure described in Preparation VIa and starting from 9.4 g (0.050 mol) of 2-bromoanisole, 1.7 g (0.069 mol) of magnesium and 11 g (0.050 mol) of 2-bromobenzoyl chloride, 9.6 g of the expected product (yield: 66%) are obtained after crystallization from ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960758 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-d2ac9a5aa2f943c19f92ca55bc0d0cbf |
| Source note | uspto-grants-1990_10 |