HuagongsheHuagongshe Chemistry Print Report · For research reference only
Einecs 211-027-4 → HCID 15718537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Einecs 211-027-4 | HCID 69401 | — |
| Reactant | HCID 15718536 | HCID 15718536 | — |
| Product | HCID 15718537 | HCID 15718537 | 65% |
Reaction Steps
Following the procedure described in Preparation IVb and starting from 13.5 g (0.049 mol) of 4-(2-methoxy-5-trifluoromethylbenzoyl)benzonitrile and 31 g (0.27 mol) of pyridinium chloride, an amount of 8.4 g of the expected product (yield: 65%) is obtained after purification by flash chromatography using a hexane/ethyl acetate mixture (5/1 v/v) as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960758 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-48f199cf1aaf4c0d82031f822262a938 |
| Source note | uspto-grants-1990_10 |