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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1087719Generated: November 2, 2026

Einecs 211-027-4 → HCID 15718537, compound

https://huagongshe.com/reaction/1087719

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEinecs 211-027-4HCID 69401—
ReactantHCID 15718536HCID 15718536—
ProductHCID 15718537HCID 1571853765%

Reaction Steps

Following the procedure described in Preparation IVb and starting from 13.5 g (0.049 mol) of 4-(2-methoxy-5-trifluoromethylbenzoyl)benzonitrile and 31 g (0.27 mol) of pyridinium chloride, an amount of 8.4 g of the expected product (yield: 65%) is obtained after purification by flash chromatography using a hexane/ethyl acetate mixture (5/1 v/v) as the eluent.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04960758
Source datasetuspto-grants-1990_10
ORD IDord-48f199cf1aaf4c0d82031f822262a938
Source noteuspto-grants-1990_10