HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octylamine → 1-(2-Hydroxyethyl)-3-octylimidazolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | 3-(2-Chloroethyl)-1,3-oxazolidin-2-one | HCID 75633 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-(2-Hydroxyethyl)-3-octylimidazolidin-2-one | HCID 14836219 | 83% |
Reaction Steps
7.1 g of 3-(2-chloroethyl)oxazolidin-2-one was treated with 12.271 g of octyl amine. The reaction mixture was stirred overnight, diluted with ethyl acetate and washed with water and brine. The organic solution was dried and concentrated to give 9.55 g (83%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960771 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-2516ec45db7847b0ac73ae7bc7c74848 |
| Source note | uspto-grants-1990_10 |