HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22163866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 22163865 | HCID 22163865 | — |
| Catalyst | Methyltriphenyliphosphonium bromide | HCID 74505 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22163866 | HCID 22163866 | — |
Reaction Steps
2-(1H-1,2,4-Triazol-1-yl)-2,2',4'-trifluoroacetophenone (10 g), anhydrous potassium carbonate (7.3 g), and methyltriphenylphosphonium bromide (15.5 g) were heated under reflux for 16 hours in 1,4-dioxan (250 ml), to which water (1.0 g) had been added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960782 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-03b76d36c6194f70b7d938ca200e7831 |
| Source note | uspto-grants-1990_10 |