Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 1-(1H-1,3-benzodiazol-5-yl)ethan-1-one | HCID 12262904 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22163881 | HCID 22163881 | — |
Reaction Steps
1.21 g (7.6 mmol) of bromine in 5 ml of glacial acetic acid are added to a solution of 1.2 g (7.5 mmol) of 5-acetylbenzimidazole and 1.35 g of 48% strength aqueous HBr (=8 mmol of HB) in 15 ml of glacial acetic acid at room temperature. The mixture is stirred at 40° C. for 30 minutes and cooled and the product which has precipitated out is filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04960783 |
|---|
| Source dataset | uspto-grants-1990_10 |
|---|
| ORD ID | ord-b1793726a0e646c58847c84ea25c9226 |
|---|
| Source note | uspto-grants-1990_10 |
|---|
