HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 86744248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 22163909 | HCID 22163909 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86744248 | HCID 86744248 | — |
Reaction Steps
A mixture of 1-(2,6-dimethylphenyl)-3-acetyl-1H-pyrrole (20.0 g), hydroxylamine hydrochloride (25.0 g), pyridine (130 ml) in 100 ml of methanol is heated under reflux for 20 hours. Workup in the usual manner yields 1-(2,6-dimethylphenyl)-3-acetyl-1H-pyrrole oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960787 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-a5951e8838f7418cb50abf68382dd20b |
| Source note | uspto-grants-1990_10 |