1-Pyrrolidineethanamine → HCID 14763444, compound

Participants

Reaction Steps

This compound was prepared according to the procedure used to synthesize the compound of Example 5. A mixture of 5.7 g (0.035 mole) of 1,1'-carbonyldiimidazole, 3.9 g (0.034 mole) of N-(2-aminoethyl)pyrrolidine, and 4.9 g (0.03 mole) of 1-phenylpiperazine in a total of 200 ml of tetrahydrofuran gave 5.4 g (59%) of the title compound as a white powder, m.p. 81.5°-84° C., after recrystallizing from diisopropyl ether.

Provenance & Evidence