1-Phenylpiperazine → HCID 14763445, compound

Participants

Reaction Steps

This compound was prepared according to the procedure used to synthesize the compound of Example 5. A mixture of 5.7 g (0.035 mole) of 1,1'-carbonyldiimidazole, 4.4 g (0.034 mole) of N-(2-aminoethyl)piperidine and 4.9 g (0.03 mole) of 1-phenylpiperazine in a total of 200 ml of tetrahydrofuran gave 2.3 g (24%) of title compound as a white solid, m.p. 64°-67° C. after recrystallization from diethyl ether.

Provenance & Evidence