1-Phenylpiperazine → HCID 14763435, compound

Participants

Reaction Steps

This compound was prepared according to the procedure used to synthesize the compound of Example 5. A mixture of 5.7 g (0.035 mole) of 1,1'-carbonyldiimidazole, 3.0 g (0.034 mole) of unsym-dimethylethylenediamine and 4.9 g (0.03 mole) of 1-phenylpiperazine in a total of 200 ml of tetrahydrofuran gave 3.6 g (43%) of title compound as a white powder, m.p. 88°-90° C., after recrystallization from diisopropyl ether.

Provenance & Evidence