HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromophenol → HCID 15058601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromophenol | HCID 7244 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoroethyl bromide | HCID 12982 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15058601 | HCID 15058601 | 77.1% |
Reaction Steps
In a manner similar to that disclosed in German Offenlegungschrift DE No. 3,402,483, the reaction of 5.0 grams (0.029 mole) of 2-bromophenol, 6.0 grams (0.043 mole) of potassium carbonate, and 5.5 grams (0.03 mole) of 1-bromo-2-fluoroethane in 50 ml of N,N-dimethylformamide yielded 4.9 grams of 2-bromophenyl 2-fluoroethyl ether as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960884 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-f94651e5f9184654b83e6f980afe9322 |
| Source note | uspto-grants-1990_10 |