HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 22164143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 11400997 | HCID 11400997 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22164143 | HCID 22164143 | 62% |
Reaction Steps
In a manner similar to that disclosed by Godfrey et al., (J. Chem. Soc. Perkin I, 1353-1354 (1974), the reaction of 10.0 grams (0.06 mole) of 2-(2-fluoroethoxy)benzaldehyde with 3-chloroperbenzoic acid (15.5 grams of 80-85% assay, 0.075 mole) in 250 ml of methylene chloride yielded 6.85 grams of 2-(2-fluoroethoxy)phenyl formate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960884 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-07f8a44267db49759cb85025f6646fe0 |
| Source note | uspto-grants-1990_10 |