HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 70358983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 22164323 | HCID 22164323 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70358983 | HCID 70358983 | 15% |
Reaction Steps
In analogy to Example 5, the N-methyl-2-N-phenylamino-4-chlorothiazole-sulphonamide was prepared by reacting N-methyl-2,4-dichlorothiazole-sulphonamide from Example 2 with aniline. Following chromatography on silica gel using methylene chloride as the eluent, the product having a melting point of 157-8° C. was obtained in 15% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960899 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-d39a86a9c6d34b69ac8ff5c15e88184a |
| Source note | uspto-grants-1990_10 |