HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 70358954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | HCID 22164323 | HCID 22164323 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 70358954 | HCID 70358954 | — |
Reaction Steps
In analogy to Example 5, the N-methyl-2-N-isopropylamino-4-chlorothiazole-sulphonamide was prepared by reacting N-methyl-2,4-dichlorothiazole-sulphomamide from Example 2 with a 65% strength aqueous isopropylamine solution. Following recrystallization from toluene, 89% yield of product of m.p. 135° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04960899 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-4b037f4d6b7a4d51b3a8184c5525fc45 |
| Source note | uspto-grants-1990_10 |