L-Phenylalanine → HCID 66996790, compound

HRID 1087983Notes

Reaction equation

HRID 1087983 reaction equation
S([O-])([O-])(=O)=O.[Zn+2:6].[NH2:7][C@H:8]([C:16]([OH:18])=[O:17])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[NH2:7][C@H:8]([C:16]([O-:18])=[O:17])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[Zn+2:6].[NH2:7][C@H:8]([C:16]([O-:18])=[O:17])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 6140L-PhenylalanineHCID 24424Zinc Sulfate

Product 1

HCID 66996790HCID 66996790, compound

Procedure

26.5 g of zinc sulfate (0.17 M) is added to 1l of fermented broth of phenylalanine (27 g/l, 0.16 M) from which the microorganisms have been removed. The mixture is stirred slowly to completely dissolve the zinc sulfate. Ammonia water is gradually added to the dissolved solution to maintain the pH of 7.5 and then zinc phenylalaninate crystals are obtained (crystal wt: 32.4 g, purity: 99.2%).

Workup

  1. customhave been removed
  2. dissolutionto completely dissolve the zinc sulfate
  3. additionAmmonia water is gradually added to the dissolved solution
  4. temperatureto maintain the pH of 7.5

Sources & evidence

ORD record
ord-64e2621fb3c741948105af6e5e1c8063
Source dataset
uspto-grants-1990_10
Patent number
US04960930

Reaction notes

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