HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54541299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | 3-(2-Quinolin-2-yl-vinyl)-phenol | HCID 4878841 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54541299 | HCID 54541299 | — |
Reaction Steps
A suspension of milled potassium carbonate (0.5 g), quinoline from Step 2 (1.1 g), and methylbromoacetate (4.0 ml) in acetone (25 ml) were refluxed overnight. The reaction mixture is poured onto water, extracted with ethyl acetate dried and evaporated. Chromatography of the residue on SiO2 using 30 to 40% ether/hexane afforded the title compound: m.p. 110-112°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962203 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-b7a841ca62e44bfca5a60744eacba619 |
| Source note | uspto-grants-1990_10 |