HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl bromoacetate → HCID 22163068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | HCID 86744273 | HCID 86744273 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 22163068 | HCID 22163068 | — |
Reaction Steps
A mixture of 3-hydroxy-5-propyl-benzaldehyde potassium carbonate (0.7 g) and methyl bromoacetate (0.8 ml) in methyl ethyl ketone (6 ml) were heated at 70° for 4 hours. The reaction was filtered and evaporated. Flash chromatography of the residue using 30% ether in hexane afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962203 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-04a35689bf03417d811827af66fd0f0c |
| Source note | uspto-grants-1990_10 |