HRID1088452

反应详情

EQUATION

反应方程式

HRID 1088452 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 3-hydroxy-5-propyl-benzaldehyde potassium carbonate (0.7 g) and methyl bromoacetate (0.8 ml) in methyl ethyl ketone (6 ml) were heated at 70° for 4 hours. The reaction was filtered and evaporated. Flash chromatography of the residue using 30% ether in hexane afforded the title compound.

WORKUP

后处理

  1. temperaturewere heated at 70° for 4 hours
  2. filtrationThe reaction was filtered
  3. customevaporated