HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 53923850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromopropionitrile | HCID 140538 | — |
| Reactant | HCID 54097337 | HCID 54097337 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 53923850 | HCID 53923850 | — |
Reaction Steps
A mixture of the phenol from Step 1 (150 g), (+) 2-bromo-propionitrile and milled potassium carbonate in methylethyl ketone (1 L) was refluxed for 8 hrs. The reaction mixture was cooled and filtered. Recrystallization from ethyl acetate/hexane afforded the title compound m.p. 118°-120°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962203 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-2c35e305da394751abb9f20d75316c7c |
| Source note | uspto-grants-1990_10 |