HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53740121, compound → HCID 13037713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53740121 | HCID 53740121 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13037713 | HCID 13037713 | 82.1% |
Reaction Steps
N-(α-methyl-p-octyl benzylidene) aniline (49 g), prepared by the procedure described in Example IA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. N-(α-methyl-p-octyl-benzyl)aniline (II) (40.5 g) was obtained by fractional distillation. The desired product II had a boiling point of 173° to 178° C. at 0.025 millimeter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-1fb98bee9ec64610a6bf4013c8224458 |
| Source note | uspto-grants-1990_10 |