HCID 53822952, compound → HCID 22163153, compound

HRID 1088501Notes

Reaction equation

HRID 1088501 reaction equation
[CH3:1][C:2](=[N:9][C:10]1[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:12][CH:11]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>[Pd].C(O)C>[CH3:1][CH:2]([NH:9][C:10]1[CH:11]=[CH:12][C:13]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:14][CH:15]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 1

HCID 53822952HCID 53822952, compound

Product 1

HCID 22163153HCID 22163153, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

N-(α-methyl benzylidene)-p-nonyl aniline (III) (16.5 g) prepared by the procedure described in Example IIA was hydrogenated suing 5% Pd/C as the catalyst and 95% ethanol as the solvent. N-(α-methyl benzyl)-p-nonyl aniline (IV) was obtained by fractional distillation. IV had a boiling point of 180°-184° C. at 0.025 millimeter.

Sources & evidence

ORD record
ord-6a2903d343d2467e8e2af12b47718db9
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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