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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1088507Generated: November 3, 2026

Benzene → HCID 22163148, compound

https://huagongshe.com/reaction/1088507

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzeneHCID 241—
ReactantBenzocaineHCID 2337—
ReactantAcetophenoneHCID 7410—
SolventWaterHCID 962—
ProductHCID 22163148HCID 22163148—

Reaction Steps

A solution of acetophenone (44 ml), ethyl-p-aminobenzoate (60 g), benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(α-methyl benzylidene)-p-carbethoxy aniline (XI). XI had a m.p. of 87° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04962234
Source datasetuspto-grants-1990_10
ORD IDord-0874799887264143894086407acce689
Source noteuspto-grants-1990_10