HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 22163148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Benzocaine | HCID 2337 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22163148 | HCID 22163148 | — |
Reaction Steps
A solution of acetophenone (44 ml), ethyl-p-aminobenzoate (60 g), benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(α-methyl benzylidene)-p-carbethoxy aniline (XI). XI had a m.p. of 87° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-0874799887264143894086407acce689 |
| Source note | uspto-grants-1990_10 |