HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22163145, compound → HCID 22163150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22163145 | HCID 22163145 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22163150 | HCID 22163150 | — |
Reaction Steps
N-(α-methyl benzylidene)m-carbethoxyaniline (27 g) prepared by the procedure described in example VIIA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. N-(α-methyl benzyl m-carbethoxy aniline (XIV) was obtained by fractional distillation. XIV had a boiling point of 156° C. at 0.1 millimeter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-4246d3f98b8f4977af70228eeef40f60 |
| Source note | uspto-grants-1990_10 |