HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 22163142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Ethyl 2-aminobenzoate | HCID 6877 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22163142 | HCID 22163142 | — |
Reaction Steps
A solution of acetophenone (100 ml), o-carbethoxyaniline (90 ml), benzene (100 ml) was refluxed in the presence of molecular sieve (40 g) with continuous removal of water. N-(α-methyl benzylidene)-o-carbethoxyaniline (XV) was obtained by fractional distillation. XV had a boiling point of 123° at 0.1 millimeter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-17198f3ec9cb4fbeb3438dcaf39855cc |
| Source note | uspto-grants-1990_10 |