Benzene → HCID 22163142, compound

HRID 1088511Notes

Reaction equation

HRID 1088511 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=O)[CH3:2].[C:10]([C:15]1[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=1[NH2:17])([O:12][CH2:13][CH3:14])=[O:11].C1C=CC=CC=1>O>[CH3:2][C:1](=[N:17][C:16]1[CH:18]=[CH:19][CH:20]=[CH:21][C:15]=1[C:10]([O:12][CH2:13][CH3:14])=[O:11])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

5

Reactant 3

HCID 241BenzeneHCID 6877Ethyl 2-aminobenzoateHCID 7410Acetophenone

Product 1

HCID 22163142HCID 22163142, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of acetophenone (100 ml), o-carbethoxyaniline (90 ml), benzene (100 ml) was refluxed in the presence of molecular sieve (40 g) with continuous removal of water. N-(α-methyl benzylidene)-o-carbethoxyaniline (XV) was obtained by fractional distillation. XV had a boiling point of 123° at 0.1 millimeter.

Sources & evidence

ORD record
ord-17198f3ec9cb4fbeb3438dcaf39855cc
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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