Benzene → HCID 13263368, compound

HRID 1088514Notes

Reaction equation

HRID 1088514 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=O)[CH3:2].[Cl:10][C:11]1[CH:12]=[C:13]([CH:15]=[CH:16][CH:17]=1)[NH2:14].C1C=CC=CC=1>O>[Cl:10][C:11]1[CH:12]=[C:13]([CH:15]=[CH:16][CH:17]=1)[N:14]=[C:1]([CH3:2])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

5

Reactant 3

HCID 241BenzeneHCID 7410AcetophenoneHCID 79323-Chloroaniline

Product 1

HCID 13263368HCID 13263368, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of acetophenone (130 ml), m-chloroaniline (130 ml) and benzene (200 ml) was refluxed in the presence of molecular sieve (50 g) with continuous removal of water. m-Chloro-N-(α-methyl benzylidene) aniline (XIX) was obtained by fractional distillation. XIX had a boiling point of 110° C. at 0.025 millimeter.

Sources & evidence

ORD record
ord-dedfce4848d649209283fdb1587cd0ed
Source dataset
uspto-grants-1990_10
Patent number
US04962234

Reaction notes

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