HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 13263368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetophenone | HCID 7410 | — |
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13263368 | HCID 13263368 | — |
Reaction Steps
A solution of acetophenone (130 ml), m-chloroaniline (130 ml) and benzene (200 ml) was refluxed in the presence of molecular sieve (50 g) with continuous removal of water. m-Chloro-N-(α-methyl benzylidene) aniline (XIX) was obtained by fractional distillation. XIX had a boiling point of 110° C. at 0.025 millimeter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-dedfce4848d649209283fdb1587cd0ed |
| Source note | uspto-grants-1990_10 |