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HRID1088518

反应详情

EQUATION

反应方程式

HRID 1088518 的结构方程式

REACTANTS

反应物

3
结构：c1ccccc1
HCID241

Benzene

C6H6

结构：Nc1ccccc1
HCID6115

Aniline

C6H7N

结构：CC(=O)c1ccc(C(C)=O)cc1
HCID13888

1,4-Diacetylbenzene

C10H10O2

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(N=C(C)c2ccccc2)cc1
HCID54464667

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A solution of p-diacetylbenzene (50 g), aniline (80 g) and benzene (120 ml) was refluxed in the presence of molecular sieve (10 g) with continuous removal of water. The crude product was crystallized from ethanol to give p-acetyl-N-(α-methyl benzylidene) aniline (XXIII). XXIII had a melting point of 205° C.

WORKUP

后处理

  1. customThe crude product was crystallized from ethanol