Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene → p-acetyl-N-(alpha-methyl benzylidene) aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | 1,4-Diacetylbenzene | HCID 13888 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | p-acetyl-N-(alpha-methyl benzylidene) aniline | HCID 54464667 | — |
반응 단계
A solution of p-diacetylbenzene (50 g), aniline (80 g) and benzene (120 ml) was refluxed in the presence of molecular sieve (10 g) with continuous removal of water. The crude product was crystallized from ethanol to give p-acetyl-N-(α-methyl benzylidene) aniline (XXIII). XXIII had a melting point of 205° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04962234 |
| 출처 데이터셋 | uspto-grants-1990_10 |
| ORD ID | ord-d201f1638125472290ebfcaa4a3cefeb |
| 출처 메모 | uspto-grants-1990_10 |