HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-acetyl-N-(alpha-methyl benzylidene) aniline → p-Acetyl-N-(alpha-methyl benzyl) aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-acetyl-N-(alpha-methyl benzylidene) aniline | HCID 54464667 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | p-Acetyl-N-(alpha-methyl benzyl) aniline | HCID 54144277 | — |
Reaction Steps
p-Acetyl-N-(α-methylbenzylidene) aniline (XXIII) (30 g) prepared by the procedure described in Example XXIXA was hydrogenated using 5% Pd/C as the catalyst and 95% ethanol as the solvent. p-Acetyl-N-(α-methyl benzyl) aniline (XXIV) was obtained by fractional distillation. XXIV had a boiling point of 165° C. at 0.1 millimeter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-3a8dfda1578a4d7d8b425c809dde6ebd |
| Source note | uspto-grants-1990_10 |