HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N-(1,2,3,4-tetrahydronaphthylidene) aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 1-Tetralone | HCID 10724 | — |
| Reactant | N-Dodecylaniline | HCID 76362 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(1,2,3,4-tetrahydronaphthylidene) aniline | HCID 11183633 | — |
Reaction Steps
A solution of α-tetralone (50 ml), dodecyl aniline (80 g) and benzene (150 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was crystallized from ethanol to give N-(1,2,3,4-tetrahydronaphthylidene) aniline (XXVI). XXVI had a melting point of 53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04962234 |
| Source dataset | uspto-grants-1990_10 |
| ORD ID | ord-e154c3d869d346daa6428db55c1f5c1a |
| Source note | uspto-grants-1990_10 |